Gravimetric Analysis of a Soluble Chloride

Objective: To perform gravimetric analysis of money chloride and auspicate the percent chloride in the experiment. Introduction: Gravimetric analysis is lascivious on the quantitative isolation of the want constituentthe analyte of interest, from the sample distribution in highly pure form or in some combined form and weighing the isolated constituent. The desired constituent is usually isolated or separated by precipitation. From the masses of sample and boil down, the percentage of the constituent in the passkey sample can be calculated. Precipitation is do by organic or inorganic precipitating agents. cardinal un wash inorganic precipitating agents are silver nitrate, which is employ to effectuate halide ions such as chloride and barium chloride, which is used to precipitate sulphate ion. In these precipitate reactions, the product is a common salt because it is form by reactions between cations and anions. The 3 major requirements for a nigh gravimetric a nalysis are: the reagent will react still with the analyte of interest to form a precipitate, it forms superstar and only if one product with the analyte and the analyte precipitates quantitatively from resolving power.

In aqueous solution silver ion undergoes the following reactions with chloride: Ag+ (aq) + Cl- (aq) ? AgCl (s) Experimental Methods: Three crucibles were soundly washed with soap and water. The cleaned crucibles were whence mounted to a dawn flask, and 2 mL of concentrated nitric stinging were allowed to soak. The acid was deadened via a gentle vacuum. This was repeated 2 to a greater extent times. The crucibles were then rinsed with deionized water. Three! portions (0.316g, 0.305g, and 0.298g) of dried chloride sample were dissolved in 3 separate 400 mL beakers in one hundred fifty mL of deionized water and 1 mL of concentrated nitric acid. The three chloride solutions were then heated, and silver nitrate solution was added in 5 mL increments (while stirring vigorously) until precipitation of the silver chloride was complete. all(prenominal) beaker was then...If you compulsion to get a full essay, order it on our website: BestEssayCheap.com

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